期刊
JOURNAL OF DISPERSION SCIENCE AND TECHNOLOGY
卷 32, 期 4, 页码 591-595出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/01932691003757363
关键词
Crystal morphology; hydrothermal; nanostructures; phosphates
资金
- National Natural Science Foundation of China [20671057]
- Program for New Century Excellent Talents in the University (P. R. China)
- Doctoral Foundation of Shandong Province [2007BS04042]
- Tianjin Normal University [5RL071]
The copper hydroxyphosphate nanostructured microspheres with uniform diameter have been achieved via a template-free hydrothermal synthetic route with ammonia as alkali and complexing agent. Powder x-ray diffraction, scanning electron microscopy, Fourier transform infrared spectrometry, and x-ray photoelectron spectroscopy were used to characterize the morphologies and structures of the products. It has been found that the morphology of the final product depends strongly on the concentrations, molar ratios of the starting reagents, and the kinds of alkali. The possible formation process of the microspheres is discussed.
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