期刊
NEW JOURNAL OF CHEMISTRY
卷 39, 期 10, 页码 7559-7562出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5nj00476d
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资金
- Royal Society
- EPSRC
- ERC
- University of Nottingham
- UK National Nuclear Laboratory
- COST
- Trinity College Dublin
- Environmental Protection Agency [EPA-2012-WRM-PhD-7]
- Engineering and Physical Sciences Research Council [EP/K024000/2, EP/F030517/1, EP/G051763/1, EP/K024000/1, EP/M027015/1] Funding Source: researchfish
- EPSRC [EP/F030517/1, EP/K024000/2, EP/K024000/1, EP/M027015/1, EP/G051763/1] Funding Source: UKRI
We report that U3O8, UO2(NO3)(2)center dot 6H(2)O, and UO2Cl2 react with hexachloropropene (HCP) to give UCl4 in 60, 100, and 92% yields, respectively, and report a protocol to recycle the HCP. This renders the preparation of UCl4 more accessible and sustainable. 2,5-Dichlorohexachlorofulvene has been identified as a significant by-product from these reactions.
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