期刊
JOURNAL OF CHROMATOGRAPHY A
卷 1219, 期 -, 页码 15-28出版社
ELSEVIER
DOI: 10.1016/j.chroma.2011.11.029
关键词
Brominated flame retardants; Analysis; Review
资金
- UK Department for Environment, Food and Rural Affairs [ME4117]
This review provides a summary of various analytical methodologies applied to the determination of novel brominated flame retardants (NBFRs) in various environmental compartments, as reported in peer reviewed literature, either in print or online, until the end of 2010. NBFRs are defined here as those brominated flame retardants (BFRs) which are either new to the market or newly/recently observed in the environment. The preparation and extraction of sediment, water, sewage sludge, soil, air and marine biota samples, the extract clean-up/fractionation and subsequent instrumental analysis of NBFRs are described and critically examined. Generally, while the instrumental analysis step mainly relies on mass-spectrometric detection specifically developed for NBFRs, and hyphenated to liquid or gas chromatography, preceding steps tend to replicate methodologies applied to the determination of traditional BFRs such as polybrominated diphenyl ethers (PBDEs) and hexabromocyclododecane (HBCD). Shortcomings and gaps are discussed and recommendations for future development are given. Crown Copyright (C) 2011 Published by Elsevier B.V. All rights reserved.
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