期刊
JOURNAL OF APPLIED POLYMER SCIENCE
卷 110, 期 3, 页码 1594-1599出版社
WILEY
DOI: 10.1002/app.28584
关键词
electrochemistry; ferrocene; epoxy compound; thermosets; crosslinking
资金
- The National Natural Science Foundation of China [20772108, 20672097]
- The China Postdoctoral Science Foundation, The Science and Technology Program of Ningbo City [20070410405]
A novel ferrocene-based epoxy compound of glycidyl ester of 1,1'-ferrocene dicarboxylate was synthesized by the reaction of 1,1'-ferrocene dicarboxylate and epichlorohydrin. The resultant epoxy compound showed an irreversible redox process in cyclic voltammetry (CV) measurement. The curing behavior of glycidyl ester of 1,1'-ferrocene dicarboxylate and dicyandiamide system was investigated by nonisothermal measurement using the Ozawa's approach with the heating rate of 5, 10, 15, and 20 degrees C/min, respectively. It was found that both the diffusion of the compound and the curing temperature have effect on the curing process, and the effect of temperature was greater. (C) 2008 Wiley Periodicals, Inc.
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