期刊
JOURNAL OF APPLIED PHYSICS
卷 111, 期 7, 页码 -出版社
AMER INST PHYSICS
DOI: 10.1063/1.3691527
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资金
- Anhui University
- National Natural Science Foundations of China [20401001, 50772001]
- Science and Technological Fund of Anhui Province for Outstanding Youth, Anhui Province [08040106822]
- Research Fund for the Doctoral Program of Higher Education of China (RFDP) [20093401110003]
A novel kind of Fe3O4 hollow spheres/reduced graphene oxide (r-GO) composites has been synthesized by a facile solvothermal method. The scanning electron microscopy and transmission electron microscopy images show bowl-like Fe3O4 hollow spheres with an average outer diameter of 395 nm and a shell thickness of 100 nm decorating on the both sides of r-GO sheets. The co-existence of both D and G peaks in Raman spectra confirms the presence of r-GO state, and an increased D/G intensity ratio of the composites suggests a substantial increase in disorder degree in the r-GO sheets due to the Fe3O4 hollow spheres anchoring on the surface. Compared to pristine r-GO, pure Fe3O4 nanoparticles, and the reported solid nano-Fe3O4/r-GO, both a wider and stronger absorption have been achieved in the frequency range of 2-18 GHz. In particular, the sample containing 30 wt.% as-synthesized hollow Fe3O4/r-GO with a coating layer thickness of 2.0 mm exhibits a maximum absorption of 24 dB at 12.9 GHz as well as a bandwidth of 4.9 GHz (from frequency of 10.8-15.7 GHz) corresponding to reflection loss at -10 dB. The measured complex relative permittivity and permeability data reveal that the enhanced microwave properties are contributed by a major improved dielectric loss and a minor magnetic loss resulting from the incorporation of hollow Fe3O4 on r-GO. (C) 2012 American Institute of Physics. [http://dx.doi.org/10.1063/1.3691527]
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