期刊
JOURNAL OF APPLIED CRYSTALLOGRAPHY
卷 43, 期 -, 页码 570-577出版社
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S0021889810008587
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-
资金
- US Department of Energy [DE-AC05-000R22725]
The macromolecular neutron diffractometer MaNDi is currently under construction at the first target station of the Spallation Neutron Source at Oak Ridge National Laboratory. This instrument will collect neutron diffraction data from small single crystals (0.1-1 mm(3)) with lattice constants between 100 and 300 angstrom, as well as data from less well ordered systems such as fibers. A focusing neutron guide has been designed to filter the high-energy neutron component of the spectrum and to provide a narrow beam with a wide spectral window and angular divergence almost insensitive to neutron wavelength. The system includes a final interchangeable section of neutron guide and two slits, which enable tuning of the horizontal and vertical beam divergence between 0.12 and 0.80 degrees (full width at half-maximum) at the sample position. This allows the trading of intensity for resolution, depending on the scientific requirements. Efforts to enhance and develop suitable high-resolution neutron detectors at an affordable price are also discussed. Finally, the parameters of the neutron guide and detectors were used to simulate diffraction from a large unit cell. (c) 2010 International Union of Crystallography Printed in Singapore - all rights reserved
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