期刊
JOURNAL OF ALLOYS AND COMPOUNDS
卷 492, 期 1-2, 页码 570-575出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2009.11.183
关键词
Nanostructures; Semiconductors; Chemical synthesis
资金
- council of University of Kashan
Different morphologies of nanostructured tin sulfide (SnS) including nanoparticles, nanosheets and nanoflowers have been prepared via a simple hydrothermal reaction between SnCl2 center dot 2H(2)O and thioglycolic acid (TGA) at relatively low temperature. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), ultraviolet-visible (UV-vis) spectroscopy, photoluminescence spectroscopy (PL), and Fourier transform infrared (FT-IR) spectra. The effect of reactant concentration, mole ratio of TGA to the Sn2+, temperature and reaction time on the morphology, particle sizes and phase of nanocrystalline SnS products has been investigated. (C) 2009 Elsevier B.V. All rights reserved.
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