期刊
JOURNAL OF ALLOYS AND COMPOUNDS
卷 481, 期 1-2, 页码 450-454出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2009.02.154
关键词
Nanostructures; Crystal growth; Scanning and transmission electron microscopy
资金
- National Natural Science Foundation of China [50862008]
- National Basic Research Program of China [2007CB936300]
- Xinjiang University [BS060110]
Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200 degrees C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80 nm to 120 nm, and from 2 mu m to 3 mu m, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed. (C) 2009 Elsevier B.V. All rights reserved.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据