期刊
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
卷 60, 期 40, 页码 10015-10026出版社
AMER CHEMICAL SOC
DOI: 10.1021/jf302944p
关键词
gingerol; shogaol; high-performance liquid chromatography; time-of-flight mass spectrometry
Liquid chromatography-time-of-flight mass spectrometry (LC-TOF/MS) was established for the simultaneous separation, identification, and quantification of gingerol-related compounds in ginger products. The established method has been shown to provide a satisfactory linearity (r > 0.999) in a wide range (5-5000 ng/mL), low limits of detection and quantification, high precision, and inter- and intraday repeatability. The detection sensitivity of gingerols and shogaols by TOF/MS was 70-100 times higher than conventional UV detection at 288 nm. In this study, 19 ginerol-related compounds in the samples were identified and quantified by the established LC-TOF/MS method. The dried ginger powder products contained the highest quantity of gingerol-related compounds (7126.3-13789.0 mu g/g), followed by fresh ginger products (2007.9-2790.0 mu g/g), powdered ginger tea products (77.29-81.75 mu g/g), and hot water ginger extracts (54.59-123.23 mu g/mL). Shogaols were not found in fresh gingers. This paper represents the first report on the LC-TOF/MS analysis for the simultaneous characterization and quantification of gingerol-related compounds in ginger products.
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