期刊
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
卷 59, 期 22, 页码 12059-12072出版社
AMER CHEMICAL SOC
DOI: 10.1021/jf202556p
关键词
red mustard green; Brassica juncea Coss variety; acylated cyanidin 3-sophoroside-5-diglucosides; acylated cyanidin 3-sophoroside-5-glucosides; acylated flavonol glycosides; hydroxycinnamic acid derivatives; UHPLC-PDA-ESI/HRMS/MSn identification
资金
- Agricultural Research Service of the U.S. Department of Agriculture
An UHPLC-PDA-ESI/HRMS/MSn profiling method was used for, a comprehensive study of the phenolic components of red mustard greens (Brassica juncea Coss variety) and identified 67 anthocyanins, 102 flavonol glycosides, and 40 hydroxycinnamic acid derivatives. The glycosylation patterns of the flavonoids were assigned on the basis of direct comparison of the parent flavonoid glycosides with reference compounds. The putative identifications were obtained from tandem mass data analysis and confirmed by the retention time, elution order, and UV-vis and high-resolution mass spectra. Further identifications were made by comparing the LTHPLC-PDA-ESI/HRMS/MSn data with those of reference compounds in the polyphenol database and in the literature. Twenty-seven acylated cyanidin 3-sophoroside-5-diglucosides, 24 acylated cyanidin 3-sophoroside-5-glucosides, 3 acylated cyanidin triglucoside-5-glucosides, 37 flavonol glycosides, and 10 hydroxycinnamic acid derivatives were detected for the first time in brassica vegetables. At least 50 of them are reported for the first time in any plant materials.
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