期刊
MOLECULES
卷 20, 期 5, 页码 9309-9325出版社
MDPI
DOI: 10.3390/molecules20059309
关键词
cyclohexane-1; 3-dione; antibacterial activity; metal complexes; mass spectra; spectroscopic characterization
资金
- Chemistry Department and Nursing Department of Mus Alparslan University, Mus, Turkey
- Chemistry Department of Inonu University, Malatya, Turkey
Some new Zn(II) and Cu(II) complexes [Cu(L-1)(OAc)(2)].H2O, [Cu(L-1)(NO3)H2O].NO3.3.5H(2)O, [Zn(L-1)(NO3)(2)].4.5H(2)O, [Zn(L-1)(OAc)(2)(H2O)(2)].3H(2)O, [Cu-2(L-2)(OAc)(4)].2H(2)O.2DMF, [Cu(L-2)(2)].2NO(3).1.5DMF.H2O, [Zn(L-2)(2)(NO3)(2)].DMF and [Zn-2(L-2)(OAc)(4)(H2O)(4)].5H(2)O; L-1 = 2-[2-(2-methoxyphenyl)hydrazono]cyclohexane-1,3-dione and L-2 = 2-[2-(3-nitrophenyl)hydrazono]cyclohexane-1,3-dione were synthesized and characterized by IR, H-1-NMR,C-13-NMR and ultraviolet (UV-Vis.) spectroscopy, elemental analysis, magnetic susceptibility, mass spectrometry and thermogravimetry-differential thermal analysis (TGA-DTA). The synthesized ligands and their complexes were tested for antibacterial activity against Escherichia coli ATCC 25922, Enterococcus faecalis ATCC 29212, Staphylococcus aureus ATCC 25923, and Salmonella typhimurium CCM 583. Some of complexes showed medium-level antibacterial activity against the test bacteria compared with ampicillin.
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