期刊
INORGANIC CHEMISTRY COMMUNICATIONS
卷 24, 期 -, 页码 32-39出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.inoche.2012.07.031
关键词
Lead(II) oxalate; Lead(II) oxide; Thermal decomposition; Three-dimensional nanostructures
资金
- University of Kashan [159183/2]
We synthesized three-dimensional cauliflower-like lead(II) oxalate (PbC2O4) nanostructures by solvothermal method and then decomposed to nano-scaled lead(II) oxide (PbO) by thermal decomposition. The PbC2O4 was decomposed at 350-600 degrees C with releasing of carbon monoxide and carbon dioxide. The experimental results indicate that acetaldehyde plays a unique role in controlling the morphologies of PbC2O4. The prepared products were characterized with XRD, SEM, EDS, TG and FT-IR spectroscopies. (C) 2012 Elsevier B.V. All rights reserved.
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