期刊
INORGANIC CHEMISTRY
卷 52, 期 5, 页码 2432-2438出版社
AMER CHEMICAL SOC
DOI: 10.1021/ic3022886
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资金
- DST through the SERB
- CSIR India
- Spanish Government [CTQ2009-06959]
A series of tetranuclear lanthanide (Ln = Tb, Dy, Ho) hydroxo clusters has been synthesized by reaction of LnCl(3)center dot 6H(2)O (Ln = Tb (1), Dy (2), Ho (3)) with o-vanilin based schiff base ligand 2-(2,3 dihydroxpropyl imino methyl) 6-methoxy phenol (H3L) in methanol and in the presence of triethylamine as base. The solid state structures of all the products were established by single crystal X-ray diffraction technique. Magnetism studies reveal that Dy-4 analogue exhibits slow magnetic relaxation at low temperatures.
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