期刊
INORGANIC CHEMISTRY
卷 49, 期 14, 页码 6375-6377出版社
AMER CHEMICAL SOC
DOI: 10.1021/ic1004962
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资金
- Department of Science and Technology, DST, New Delhi, India [SR/S1/IC-19/2006]
- University Grants Commission
- Council of Scientific and Industrial Research, India
The addition of LiBH4 center dot THF to (CpTaCl4)-Ta-star (1; Cp-star = eta(5)-C5Me5) at -40 degrees C, followed by mild pyrolysis with excess BH3 center dot THF, results in the formation of the mu-acyl complex ((CpTa)-Ta-star)(2)B4H8(mu-eta(2)-COCH3) (2). The title compound represents a novel class of mu-acyl complexes in which the bicapped-tetrahedral unit ((CpTa)-Ta-star)(2)B4H8 is bridged by a mu-eta(2)-COCH3 acyl ligand.
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