期刊
HETEROCYCLES
卷 96, 期 9, 页码 1622-1630出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.3987/COM-18-13953
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An efficient method for the synthesis of (E)-1,2-dichloro- 1-phenoxyethenes 2 has been developed. The reaction of phenol derivatives 1 with trichloroethylene at ambient temperature by means of Cs2CO3-DMSO system furnished the corresponding aryl vinyl ethers 2 in excellent yields. On the other hand, the same reaction of phenol derivatives li, 1k and 1p possessing an electron-withdrawing group at the o- or p-position of the hydroxy group required a harsh reaction conditions to heat at 70 degrees C for the synthesis of the desired products 2i, 2k and 2p.
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