期刊
HETEROCYCLES
卷 80, 期 2, 页码 1003-1012出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.3987/COM-09-S(S)75
关键词
(+/-)-Heliannuol D; (+/-)-10-epi-Heliannuol D; Total Synthesis; Platinum Catalyzed Addition; Allene
资金
- Program for the Promotion of Basic and Applied Research for Innovations in the Bio-oriented Industry (BRAIN)
An alternative total synthesis of (+/-)-heliannuol D has been achieved in 13 steps and 6.9% overall yield from the arylboronic acid 9. The synthesis applies the previously developed regiocontrolled addition of arylboronic acids to allenes using a platinum catalyst to install the C5 carbon chain on the aryl ring.
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