Journal
GREEN CHEMISTRY
Volume 15, Issue 1, Pages 177-180Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2gc36711d
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Funding
- EPSRC DICE project
- Royal Society Wolfson Merit Award
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The oxidation of an allylic alcohol to its hydroperoxides represents a key step in the synthesis of a series of spirobicyclic, antimalarial trioxanes. Herein, we investigate the continuous photo-oxidation of an allylic alcohol with O-1(2) in scCO(2), as a 'green' alternative to conventional methods, and examine the remaining two steps in the synthesis of antimalarial trioxanes from readily available starting materials.
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