Journal
GREEN CHEMISTRY
Volume 14, Issue 7, Pages 1859-1863Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2gc35305a
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An efficient and widely applicable preparation of gamma-hydroxy-alpha,beta-acetylenic esters is described by means of a one-pot dehydrobromination of a 2-bromoacrylate ester with LTMP followed by the electrophilic addition of the transient propiolate to different aldehydes in the eco-friendly solvent 2-MeTHF.
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