Journal
GREEN CHEMISTRY
Volume 14, Issue 2, Pages 378-392Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1gc15925a
Keywords
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Funding
- Alexander von Humboldt Foundation
- University of Regensburg
- Spanish National Research Council (CSIC) [PIE 200980I059]
- UGC (India)
- TSRI
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The effectiveness of neutral pH chitosan hydrogel beads (CSHB) as a green organocatalyst for a variety of C-C bond forming reactions (i.e. aldol reaction, Knoevenagel condensation, nitroaldol (Henry) reaction, Michael addition) has been comprehensively evaluated. Reaction rates, conversions and selectivities were studied as a function of a series of input variables including size, pH and reactive surface area of the beads, catalyst loading, temperature, molecular weight of the biopolymer, concentration, solvent system and molar ratio of reactants. Moreover, the catalytic biohydrogel beads were characterized by a variety of techniques including, among others, SEM, FT-IR, TGA and DSC.
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