4.4 Article

Experience of the International Association of Geoanalysts as a Certifying Body

Journal

GEOSTANDARDS AND GEOANALYTICAL RESEARCH
Volume 34, Issue 3, Pages 215-230

Publisher

WILEY
DOI: 10.1111/j.1751-908X.2010.00074.x

Keywords

certifying body; certified reference materials; uncertainty; traceability; chemical composition; analytical bias; organisme de certification; materiaux de reference certifies; incertitude; tracabilite; composition chimique; biais d'analyse

Funding

  1. Geoanalysis 2009 organising committee

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Reference materials (RMs) to support geoanalysis have a long history, dating back to the issuance of G-1 and W-1 in 1951. This paper addresses only one aspect of the most recent part of that history, the experience of the International Association of Geoanalysts (IAG) as a certifying body. In 2002, the Certification Committee of the IAG met in Potsdam to discuss becoming a certifying body able to produce RMs for the geoanalytical community. Following that meeting, the IAG developed and published a protocol to assure that IAG RMs would meet International Organization for Standardization (ISO) guidelines to the fullest extent possible. Many practical problems arise in the application of the recommendations of the ISO Guides to any one specific certification project. The recommendations describe the ideal; achievable reality is always somewhat less than that ideal, presenting a significant challenge to the IAG as a certifying body. This paper will summarise experience to date, while focusing on the most challenging issues, deriving uncertainties compliant with the Guide to Uncertainty in Measurement (GUM) and establishing traceability of certified values (CVs).Les materiaux de reference servant de support au programme 'Geoanalysis' ont une longue histoire, remontant a l'emission de G-1 et W-1 en 1951. Le present article ne porte que sur un aspect de la partie la plus recente de cette histoire, l'experience de l'Association internationale des Geoanalystes (IAG) comme organisme de certification. En 2002, le Comite de certification de l'IAG s'est reuni a Potsdam pour discuter de son evolution comme organisme de certification en mesure de produire des materiaux de reference pour la communaute des geoanalytistes. Suite a cette reunion, l'IAG a elabore et publie un protocole pour garantir que les materiaux de reference IAG etaient le plus possible en accord avec les directives de l'Organisation internationale de normalisation (ISO). De nombreux problemes pratiques se posent dans l'application des recommandations des guides ISO a tout projet de certification specifique. Les recommandations decrivent l'ideal, la realite pouvant etre atteinte etant toujours un peu eloignee de cet ideal, et representent donc un defi important pour l'IAG en temps qu'organisme de certification. Cet article resume l'experience acquise jusqu'ici, tout en se concentrant sur les questions les plus difficiles, decoulant des incertitudes compatibles avec le Guide de l'incertitude dans la mesure (GUM) et de l'etablissement de la tracabilite des valeurs certifiees (CVs).

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