Journal
FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES
Volume 20, Issue 2, Pages 99-108Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/1536383X.2010.533300
Keywords
Fullerene; microwave; aza-fullerene; synthesis; mass spec
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Funding
- Valdosta State University chemistry department
- NSF-NUE
- VSU-QEP
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0911080] Funding Source: National Science Foundation
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1126587] Funding Source: National Science Foundation
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In this paper, it is reported that microwave synthesis techniques can be used to convert graphite powder and fluorinated graphite in different matrices to fullerenes (i.e., C-60 and C-70). The microwave approach allows for the quick, economical production of the carbon allotropes. Matrix Assisted Laser Desorption Ionization Time of Flight Mass (MALDI-TOF) spectrometry is used as the detection technique. Pyrrole was also used as a reactant and the formation of aza-fullerenes was suggested by the mass spectral data.
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