Journal
FORENSIC SCIENCE INTERNATIONAL
Volume 216, Issue 1-3, Pages 19-28Publisher
ELSEVIER IRELAND LTD
DOI: 10.1016/j.forsciint.2011.08.011
Keywords
Forensic; Methcathinone; Drug; 2,3-Isomers; Synthesis; Analysis
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The first synthesis of the 2,3-isomers of MDPV, butylone and methylone is reported. The isomers were characterised by H-1 and C-13 NMR spectroscopy and compared to the corresponding 3,4-isomers. A GC method is described which separates the 3,4- and the 2,3-isomers from each other. IR spectra of the 2,3-isomers are also compared with the corresponding 3,4- isomers. Two seized drug samples were analysed by GCMS and the samples were found to contain the 3,4-isomers. (C) 2011 Elsevier Ireland Ltd. All rights reserved.
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