Journal
FOOD ANALYTICAL METHODS
Volume 7, Issue 7, Pages 1381-1386Publisher
SPRINGER
DOI: 10.1007/s12161-013-9760-z
Keywords
Hollow fiber liquid phase microextraction; Graphene; Bisphenol A; 4-Tert-butylphenol; High-performance liquid chromatography
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Funding
- National Natural Science Foundation of China [31171698]
- Science and Technology Supporting Program of Hebei Province [12396908D]
- Natural Science Foundation of Hebei Province [B2012204028]
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A new analytical method by graphene-reinforced hollow fiber liquid-phase microextraction combined with high-performance liquid chromatography fluorescence detection was developed for the determination of bisphenol A and 4-tert-butylphenol in bottled juices. Several important experimental parameters were studied to get optimal extraction conditions for the analytes. Under the optimized conditions, the method showed a good performance having a linear response in the range from 0.05 to 10.0 ng mL(-1) with the correlation coefficients (r) of 0.9965-0.9994 and limits of detection of 0.01 ng mL(-1). The relative standard deviations were in the range from 6.4 to 7.2 % at the spiked concentration of 1.0 ng mL(-1). The method combines the high-adsorption capacity of graphene and the excellent clean-up performance of hollow fiber liquid-phase microextraction and has been successfully applied to the analysis of the analytes in bottled juice samples.
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