Journal
EUROPEAN POLYMER JOURNAL
Volume 44, Issue 7, Pages 2236-2243Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.eurpolymj.2008.04.037
Keywords
polyamideimide; silica; hybrid; compatibilized; microstructure
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In this work, we prepared and characterized polyamideimide (PAI)/silica hybrids compatibilized with 3-aminopropyltriethoxysilane (APTES). PAI/silica nanohybrid thin films were prepared using an in situ sot-gel process, followed by thermal imidization. We have investigated the microstructures and properties of the PAI/silica hybrids using FT-IR spectroscopy, X-ray diffraction, small-angle X-ray scattering (SAXS), and differential scanning calorimetry (DSC). We also measured their tensile properties, thermal properties, refractive indices, and dielectric constants. In general, the properties of the PAI/silica hybrids were optimized when the silica content was 6 wt.%. (c) 2008 Elsevier Ltd. All rights reserved.
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