Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 137, Issue 28, Pages 8928-8931Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jacs.5b05735
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Funding
- NSFC [21332005, 21232004, 21272095, 21472071]
- PAPD of Jiangsu Higher Education Institutions
- Qing Lan Project [12QLG006]
- Outstanding Youth Fund of JSNU [YQ2015003]
- Robert A. Welch Foundation (USA) [D-1361]
- NIH (USA) [R33DA031860]
- NSF of JSNU [14XLR005]
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A catalytic domino spirocyclization of 1,7-enynes with simple cycloalkanes and Cyclo-1,3-dicarbonyls has been established via multiple C-C bond formations from alkynyl/alkenyl functions and dual alpha,alpha-C(sp(3))-H abstractibn/insertion The reaction involves addition, 6-exo-dig cyclization and radical coupling sequences under convenient catalytic conditions and provides a concise access to spiro cyclopenta[c]quinolines in good to excellent yields.
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