Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2014, Issue 26, Pages 5735-5748Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201402672
Keywords
Total synthesis; Natural products; Alkaloids; Nitrogen heterocycles; Cyclization; Palladium
Categories
Funding
- National Natural Science Foundation of China (NSFC) [21372017, 21290183]
- National Basic Research Program of China (973 Program) [2010CB833200]
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A full account of the concise total syntheses of dictyodendrins B and E, and the formal synthesis of dictyodendrin C are described. A palladium-catalysed Larock indole synthesis was used to form the highly substituted indole core, and a palladium-mediated one-pot consecutive Buchwald-Hartwig amination/C-H activation reaction was used to construct the key pyrrolo[2,3-c]carbazole core. Unsuccessful synthetic strategies are also discussed.
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