Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2014, Issue 16, Pages 3319-3322Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201402077
Keywords
Palladium; Solvent-free reactions; Cross-coupling; Amination; Palladium
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Funding
- Russian Foundation for Basic Research (RFBR) [13-03-1224013 ofi_m]
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A highly efficient solvent-free protocol for the Buchwald-Hartwig amination of (hetero)aryl halides by secondary amines was developed. The reaction is mediated by a Pd(OAc)(2)/RuPhos catalytic system in air. Various (hetero) aryl halides were coupled with diaryl, alkyl-aryl, and dialkylamines in good to excellent yields (51 examples, 50-99% yield).
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