Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2013, Issue 20, Pages 4319-4324Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201300253
Keywords
Synthetic methods; Amines; Cleavage reactions; Reduction; Diastereoselectivity
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Funding
- Department of Science AMP
- Technology (DST), New Delhi
- Council of Scientific and Industrial Research (CSIR)
- University Grants Commission (UGC)
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A scalable approach to the syntheses of enantiomerically pure cis-1,2-cyclohexanediamines as well as exo- and endo-7-azabicyclo[2.2.1]heptan-2-amines is reported that utilizes meso-tert-butyl 2,3-bis(phenylsulfonyl)-7-azabicyclo[2.2.1]hept-2-ene-7-carboxylate as a starting material.
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