Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2013, Issue 14, Pages 2922-2929Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201201682
Keywords
Henry reaction; CC coupling; -Nitro alcohols; Asymmetric synthesis; Diastereoselectivity
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Funding
- Department of Science and Technology (DST), New Delhi [SR/S1/OC-25/2007]
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An efficient method for the synthesis of -nitro alcohols from nitro alkanes and aldehydes in aqueous phosphate buffer under neutral pH conditions at room temperature is reported. In the case of higher nitro alkanes, the reaction showed very good diastereoselectivity to give syn -nitro alcohols in preference to their anti products.
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