Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2013, Issue 24, Pages 5247-5250Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201300473
Keywords
Synthetic methods; Cross-coupling; Radical reactions; Trifluoromethylation; Iron
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Funding
- Department of Science and Technology (DST), New Delhi [R/S1/IC-24/2011]
- University Grant Commission (UGC), New Delhi
- Council of Scientific and Industrial Research (CSIR), New Delhi
- Department of Science and Technology (DST)
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A sustainable FeCl3-mediated method has been developed for the decarboxylative trifluoromethylation of ,-unsaturated carboxylic acids by using NaSO2CF3 as an economic and stable CF3 source. The reaction proceeds under mild condition and tolerates various functional groups. Advantageously, this method does not require an inert atmosphere and proceeds well in air at ambient temperature.
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