Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2012, Issue 12, Pages 2338-2345Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201200093
Keywords
Annulation; Diazo compounds; Microwave chemistry; Nitrogen heterocycles; Domino reactions
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Funding
- Aix-Marseille Universite
- Centre National de la Recherche Scientifique (CNRS)
- Departamento Administrativo de Ciencia, Tecnologia e Innovacion (COLCIEN-CIAS)
- Universidad del Valle
- Ecole Normale Superieure (ENS) Cachan
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The microwave irradiation of a series of 2-diazo-1,3-diketones in the presence of an o-phenylenediamine derivative triggered a domino Wolff rearrangement/nucleophilic addition/intramolecular imination sequence to provide a new synthetic entry to 1,3-dihydr-2H-1,5-benzodiazepin-2-ones, a class of molecules with important biological properties.
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