Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2012, Issue 8, Pages 1626-1632Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201101786
Keywords
Heterocycles; Copper; Nitriles; Tandem reactions
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Funding
- National Natural Science Foundation of China [20972124, 21103137]
- China Postdoctoral Science Foundation [20110491677]
- Xi'an City Science and Technology Project [CXY1123(1)]
- Chinese National Innovation Experiment Program for University Students [20101069702]
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Tandem reactions of nitriles with 2-aminoethanethiol hydrochloride or amino alcohols in the presence of a catalytic amount of cupric methacrylate ((Cu2L4)-L-II, L = methacrylate) were employed to prepare 2-thiazolines and 2-oxazolines under mild reaction conditions. The synthetic procedure showed high selectivity for the synthesis of mono- and bis-thiazolines and oxazolines, and a variety of 2-thiazolines and 2-oxazolines was obtained in good to excellent yields.
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