Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2011, Issue 20-21, Pages 3690-3694Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201100360
Keywords
Hypervalent compounds; Alkynes; Iodine; Iodonium salts; Benziodoxolones
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Funding
- Swedish Research Council
- Wenner-Gren Foundations
- K & A Wallenberg Foundation
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The first direct synthesis of an alkynyl(phenyl) iodonium salt from iodobenzene and an unprotected alkyne is described. The synthesis of the corresponding alkenyl(phenyl) iodonium salt is achieved from the TMS-alkyne, simply by means of changing the solvent. The one-pot synthesis of 1-arylbenziodoxolones and other iodine(III) compounds from iodine(I) precursors is also presented.
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