Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2009, Issue 9, Pages 1321-1325Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200900077
Keywords
Flow chemistry; High-temperature reactions; Microreactors; Process intensification; Supercritical fluids; Microwave chemistry
Categories
Funding
- Christian Doppler Society (CDG)
- Higher Education Commission of Pakistan
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High-temperature organic synthesis can be performed under continuous-flow conditions in a stainless steel microtubular flow reactor capable of achieving temperatures of 350 degrees C and 200 bar. Under these extreme experimental environments transformations normally performed in a high-boiling solvent at reflux temperature - or under sedled-vessel microwave conditions - can be readily converted to a flow regime by using lower boiling solvents in or near their supercritical state. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2009)
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