Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2008, Issue 20, Pages 3506-3512Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200800253
Keywords
kinetic resolution; biocatalysis; enzymes; racemization; amino acids
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A convenient procedure for the racemization of alpha-amino acid esters in the presence of catalytic amounts of salicylaldehydes is described. The combination of this racemization protocol with lipase-catalyzed ester hydrolysis allows successful dynamic kinetic resolution of various a-amino acid esters. The corresponding alpha-amino acids are obtained in high yield and optical purity. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008).
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