Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2008, Issue 30, Pages 5107-5111Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200800629
Keywords
Amines; Nucleophilic addition; Titanium tetra isopropoxide; Grignard reagents
Categories
Funding
- Merck KGaA
- Darmstadt
- KAdemCustomChem GmbH, Gottingen
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A number of tertiary sec-alkylamines (22 examples, 29-80% yield) have been prepared according to a simple one-pot procedure by the addition of Grignard reagents to N,N-dialkylformamides in the presence of Ti(OiPr)(4) and Me3SiCl. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)
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