Journal
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
Volume -, Issue 24, Pages 3789-3794Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejic.201000486
Keywords
Metal-organic frameworks; Iron; Microporous materials; Redox activity; Polymorphism
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Funding
- Ministere de l'Education Nationale, de la Recherche et de la Technologic [MENRT]
- Centre National de la Recherche Scientifique [CNRS]
- Agence Nationale de la Recherche [ANR]
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A new porous Fe-III-based MOF, formulated Fe(OH)(BDC)center dot (dmf)(x) with x approximate to 1.1 and presenting the MIL-68 topology, was prepared by reaction of an iron(III) salt and terephthalic acid (H2BDC) in N,N'-dimethylformamide (dmf) under acidic conditions. The structure and properties of this solid were studied by means of X-ray diffraction, thermogravimetric analysis, nitrogen sorption, Fe-57 Mossbauer spectrometry, and electrochemical lithium insertion.
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