Journal
JOURNAL OF SULFUR CHEMISTRY
Volume 37, Issue 1, Pages 1-13Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/17415993.2015.1082181
Keywords
trans-3,5-dihydroperoxy-3,5-dimethyl-1,2-dioxolane; DHPODMDO; oxidation; desulfurization; thioureas; thiobarbituric acid; urea
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Funding
- Research Council of Bu-Ali Sina University
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An efficient and facile procedure using trans-3,5-dihydroperoxy-3,5-dimethyl-1,2-dioxolane has been developed for oxidative desulfurization of thioureas and thiobarbituric acids. The reactions proceeded smoothly very fast under mild conditions in basic media at room temperature to afford the respective ureas in excellent yields. Simple procedure and work up, mild conditions, high yields, short reaction times, use of highly potent and non-toxic oxidant are the main merits of the present method. [GRAPHICS] .
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