Journal
JOURNAL OF SEPARATION SCIENCE
Volume 38, Issue 8, Pages 1388-1393Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201400951
Keywords
Aquatic products; Formaldehyde; Intercalative adsorbent; Polypyrrole; Thermal desorption
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Funding
- National Natural Science Foundation of China [21275168, 21127008, 21475154]
- National Key Scientific Instrument and Equipment Development Project [2011YQ03012409]
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An in situ embedded synthesis strategy was developed for the preparation of a MoO3/polypyrrole intercalative sampling adsorbent for the separation and analysis of trace volatile formaldehyde in aquatic products. Structural and morphological characteristics of the MoO3/polypyrrole intercalative adsorbent were investigated by a series of characterization methods. The MoO3/polypyrrole sampling adsorbent possessed a higher sampling capacity and selectivity for polar formaldehyde than commonly used commercial adsorbent Tenax TA. Finally, the MoO3/polypyrrole adsorbent was packed in the thermal desorption tube that was directly coupled to gas chromatography with mass spectrometry for the analysis of trace volatile formaldehyde in aquatic products. Trace volatile formaldehyde from real aquatic products could be selectively sampled and quantified to be 0.43-6.6 mg/kg. The detection limit was achieved as 0.004 mu g/L by this method. Good recoveries for spiked aquatic products were achieved in range of 75.0-108% with relative standard deviations of 1.2-9.0%.
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