Journal
ENERGY & ENVIRONMENTAL SCIENCE
Volume 4, Issue 11, Pages 4560-4566Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1ee01501j
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Funding
- U.S. Department of Energy (DOE)
- Office of Vehicle Technologies (through the Batteries for Advanced Transportation Technologies program at Lawrence Berkeley National Laboratory)
- Office of Electricity Delivery and Energy Reliability (OE)
- DOE's Office of Biological and Environmental Research
- Battelle Memorial Institute for DOE [DE-AC05-76RL01830]
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Electrochemically active LiMnPO4 nanoplates at lithiated/delithiated state were subjected to thermal stability and phase transformation evaluations for safety as a cathode material for Li-ion batteries. The phase transformation and oxygen evolution temperature of delithiated MnPO4 were characterized using in situ hot-stage X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), thermogravimetric-differential scanning calorimetry-mass spectroscopy (TGA-DSC-MS), transmission electron microscopy and scanning electron microscopy (SEM)-energy dispersive X-ray analysis (EDAX).
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