Journal
ELECTROCHIMICA ACTA
Volume 56, Issue 5, Pages 2411-2419Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.electacta.2010.10.090
Keywords
Folic acid; Vitamins; Voltammetry; Mercury meniscus modified silver solid; amalgam electrode; Hanging mercury drop electrode
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Funding
- Ministry of Education, Youth and Sports of the Czech Republic by the Research Centre [LC06035, MSM 0021627502]
- Grant Agency of Academy of Sciences of the Czech Republic [IAA400400806]
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Voltammetric behavior of folic acid and folates has been investigated using direct current voltammetry, differential pulse voltammetry and adsorptive stripping differential pulse voltammetry at a mercury meniscus modified silver solid amalgam electrode (m-AgSAE). The optimum conditions have been found for their determination in a 1:9 mixture of methanol and aqueous acetate buffer, with the limit of detection about 0.5 nmol L-1. RSD at this concentration level amounted to less than 4%. Practical applicability of the newly developed method was verified by analysis of three vitamin preparations and of two multivitamin juices. (C) 2010 Elsevier Ltd. All rights reserved.
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