Journal
ELECTROCHIMICA ACTA
Volume 56, Issue 11, Pages 4384-4389Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.electacta.2010.12.066
Keywords
Carboxylation; Allylic acetates; Carboxylic acids; Carbon dioxide; Electrosynthesis
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The electrochemical carboxylation of a series of allylic acetates and carbonates was carried out in the presence of CO2 under atmospheric pressure, with a catalytic amount of nickel-bipyridine complex, to afford the corresponding beta,gamma-unsaturated carboxylic acids. In the absence of nickel catalyst, alcohols were obtained. (C) 2011 Elsevier Ltd. All rights reserved.
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