4.6 Article

Analysis of triple phase contact in Ni-YSZ microstructures using non-destructive X-ray tomography with synchrotron radiation

Journal

ELECTROCHEMISTRY COMMUNICATIONS
Volume 12, Issue 8, Pages 1021-1024

Publisher

ELSEVIER SCIENCE INC
DOI: 10.1016/j.elecom.2010.05.014

Keywords

Tomography; Solid oxide fuel cell; Synchrotron

Funding

  1. U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-AC02-06CH11357]
  2. UK EPSRC
  3. EPSRC [EP/F009720/1, EP/F007906/1] Funding Source: UKRI
  4. Engineering and Physical Sciences Research Council [EP/F007906/1, EP/F009720/1] Funding Source: researchfish

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Here, we demonstrate the use of X-ray absorption edge spectroscopy in conjunction with high resolution Xray nano-computed tomography to provide a comprehensive microstructural map of a Ni-YSZ electrode from a Solid Oxide Fuel Cell. The experimentally derived microstructure has been used to develop a geometrical test for microstructural homogeneity. (C) 2010 Elsevier By. All rights reserved.

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