Journal
ELECTROCHEMISTRY COMMUNICATIONS
Volume 12, Issue 6, Pages 820-822Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.elecom.2010.03.042
Keywords
Soft X-ray absorption spectroscopy; In situ; Cyclic voltammetry; Corrosion; Copper
Categories
Funding
- Office of Naval Research [N00014-08-1-0732]
- Office of Science, Office of Basic Energy Sciences, Chemical Sciences, Geosciences, and Biosciences Division, of the Department of Energy [DE-AC02-05CH11231]
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A novel electrochemical setup has been developed for soft X-ray absorption studies of the electronic structure of electrode materials during electrochemical cycling. In this communication we illustrate the operation of the cell with a study of the corrosion behavior of copper in aqueous NaHCO3 solution via the electrochemically induced changes of its electronic structure. This development opens the way for in situ investigations of electrochemical processes, photovoltaics, batteries, fuel cells, water splitting, corrosion, electrodeposition, and a variety of important biological processes. (C) 2010 Elsevier B.V. All rights reserved.
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