Journal
ELECTROANALYSIS
Volume 26, Issue 5, Pages 1039-1044Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.201300636
Keywords
Cyclic voltammetry; Acrylamide; Screen printed electrodes; Electroadsorption
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Funding
- Mexican Council for Science and Technology (CONACyT)
- AVANSENS program from the Community of Madrid [P2009/PPQ-1642]
- Spanish Ministry of Economy and Competitiveness [CTQ2011-28135]
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Acrylamide (AA) was electrochemically detected and quantified by means of its voltammetric response on carboxylic modified Single-Walled Carbon Nanotube Screen Printed Electrodes (COOH-SWCNT-SPEs). The electroreduction signal of AA was proportional to AA concentration at low values (below 300 mu M) and the observed sensitivity was explained in terms of AA adsorption on the COOH-SWCNT-SPEs that was demonstrated using the electrochemical response of [Fe(CN)(6)](3-) and [Fe(CN)(6)](4-) and Raman spectroscopy experiments. In order to test the suggested analytic approach (LOD of 0.03 mu M, LOQ of 0.04 mu M), detection and quantification of AA in fried potatoes was carried out using the proposed electrochemical method and HPLC. Both techniques showed similar contents of AA.
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