Journal
ELECTROANALYSIS
Volume 25, Issue 6, Pages 1446-1452Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.201200625
Keywords
Bismuth-antimony film; Screen-printed electrodes; Stripping voltammetry; Lead(II) detection
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Funding
- Science and Technology Commission of Shanghai Municipality [10391901600]
- Ministry of Education of the People's Republic of China [WK1014051]
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This work presents a disposable bismuth-antimony film electrode fabricated on screen-printed electrode (SPE) substrates for lead(II) determination. This bismuth-antimony film screen-printed electrode (Bi-SbSPE) is simply prepared by simultaneously in situ depositing bismuth(III) and antimony(III) with analytes on the homemade SPE. The Bi-SbSPE can provide an enhanced electrochemical stripping signal for lead(II) compared to bismuth film screen-printed electrodes (BiSPE), antimony film screen-printed electrodes (SbSPE) and bismuth-antimony film glassy carbon electrodes (Bi-SbGC). Under optimized conditions, the Bi-SbSPE exhibits attractive linear responses towards lead(II) with a detection limit of 0.07 mu g/L. The Bi-SbSPE has been demonstrated successfully to detect lead in river water sample.
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