Journal
JOURNAL OF PHYSICAL CHEMISTRY C
Volume 119, Issue 22, Pages 12581-12588Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.jpcc.5b02187
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Funding
- European Union (European regional development fund)
- Ministry of Science and Art of Saxony (SMWK)
- Dr.-Erich-Kruger-Foundation
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Starting from nanocrystalline and submicron wurtzite-aluminum nitride (w-AlN) powder rocksalt structure (rs-AlN) samples were synthesized by two different methods of shock wave recovery experiments. The resulting samples contained up to 86% rs-AlN, stable at room temperature, giving for the first time the possibility to comprehensively characterize the material by powder X-ray diffraction, Fourier transform infrared (IR), Raman, and Al-27 NMR spectroscopy. Raman and IR modes were calculated by density functional theory, allowing for the interpretation of the respective experimental spectra. By Al-27 NMR the chemical shift of rs-AlN was determined, and the quadrupolar coupling constant was estimated.
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