Journal
DYES AND PIGMENTS
Volume 99, Issue 3, Pages 748-752Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.dyepig.2013.06.018
Keywords
Hydrogen sulfide; Colorimetry; Probe; Reduction; Nitrobenzoxadiazole derivative; Selenoether
Funding
- Chung-Ang University
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A new reaction-based probe for the colorimetric signaling of hydrogen sulfide was developed. Reduction of the nitro group of a nitrobenzoxadiazole moiety to an amino group resulted in pronounced chromogenic signaling in the form of a yellow to pink color change. The transformation of the nitro group to amino group was confirmed by the H-1 NMR spectroscopy. The seleno derivative showed more efficient signaling behavior than the phenylthio and phenoxy analogues. Hydrogen sulfide signaling of phenylseleno-nitrobenzoxadiazole probe was fast and completed immediately after sample preparation. Selective signaling of hydrogen sulfide was possible in the presence of commonly encountered metal ions and anions with a detection limit of 2.1 x 10(-6) M. (C) 2013 Elsevier Ltd. All rights reserved.
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