Journal
JOURNAL OF ORGANOMETALLIC CHEMISTRY
Volume 783, Issue -, Pages 92-95Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jorganchem.2015.02.028
Keywords
Zinc; beta-Diketiminate; Sulfur
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Funding
- University of Duisburg-Essen
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The homoleptic thio-beta-ketiminate zinc complex [MesNC(Me)CH{C(Me)NMes}S](2)Zn (1) was obtained from reactions of elemental sulfur with the beta-diketiminato zinc complexes [CH{C(Me)NMes}(2)]ZnMe, [CH {C(Me)NMes}(2)](2)Zn-2 and [[CH{C(Me)NMes}(2)]Zn-TePh](2). 1 and the byproducts were characterized by multinuclear NMR (H-1, C-13, Te-125) and IR spectroscopy, elemental analyses as well as by single crystal X-ray diffraction. (C) 2015 Published by Elsevier B.V.
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