Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 9, Pages 4697-4703Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b00558
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Funding
- Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry
- Priority Academic Program Development of Jiangsu Higher Education Institutions
- Key Laboratory of Organic Synthesis of Jiangsu Province
- PSC- CUNY from the City University of New York [67312-0045]
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A new approach to the selective synthesis of (E)-vinyl sulfones has been developed via a Fe/Cu co-catalyzed sulfonylation of arylpropiolic acid or phenylacetylene with sulfonyl hydrazides. A variety of vinyl sulfones have been obtained in moderate to good yields, comparable to the best results reported so far. The inexpensive Fe/Cu co-catalyzed method features a simple experimental procedure and good tolerance of substrate.
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